The Determination of Capillary Properties of Finely Porous Medium by the Water Crystallization Onset

Tyumen State University Herald. Physical and Mathematical Modeling. Oil, Gas, Energy


Release:

2016, Vol. 2. №1

Title: 
The Determination of Capillary Properties of Finely Porous Medium by the Water Crystallization Onset


About the authors:

Zoya A. Ishkova, Associate, Earth Cryosphere Institute, Tyumen Scientific Centre of the Siberian Branch of the Russian Academy of Sciences; z.ishkova@yandex.ru

Vladimir S. Kolunin, Dr. Sci. (Geol.-Mineral.), Professor, Department of Earth Cryology, Industrial University of Tyumen; Earth Cryosphere Institute, Tyumen Scientific Centre of the Siberian Branch of the Russian Academy of Sciences; askold@ikz.ru

Abstract:

This paper presents the results of a study of capillary properties of water-saturated porous ceramics from ice and air penetration through it. A method for determining the maximal size of the through pore based on the measurement of temperature of water crystallization onset is described. The temperature at which ice penetrates into the ceramics, the temperature of crystallization onset, and the maximum size of the through channel by the bubble point method were experimentally determined. The correlation dependence between the temperature of ice penetration and gas pressure at the bubble point was constructed on the experimental data. The obtained value of the surface tension coefficient of “water-ice” (0,039 J/m2) is in good agreement with the results published earlier.

References:

  1. Cheremskoi P. G. 1985. Metody issledovaniya poristosti tverdykh tel [Research Methods of Solid Body Porosity]. Moscow: Energoatomizdat.
  2. Desyatov A. V., Izvolskii I. M. 2005. Russian Federation Patent no 2248552 “Sposob opredeleniya maksimalnogo razmera por membrany metodom puzyrka” [A Method for Determining the Maximum Pore Size of the Membrane by Bubble Sort Method], March 20.
  3. Ershova E. D. (ed.). 2001. Osnovy geokriologii. Ch. 4. Dinamicheskaya geokriologiya [Fundamentals of Geocryology. Part 4. Dynamic Geocryology]. Moscow: Moscow State University Publishing House.
  4. Gorelik Ya. B., Kolunin V. S. 2002. Fizika i modelirovanie kriogennykh protsessov v litosfere [Physics and Modeling of Cryogenic Processes in the Lithosphere]. Novosibirsk.
  5. GOST R 50516-93. 1993. Membrany polimernye. Metod opredeleniya tochki puzyrka ploskikh membrane [Polymer membranes. Membrane Bubble Point Determination Technique]. Moscow: Gosstandart Rossii.
  6. Kolunin V. S., Gubarkova Z. A., Kolunin A. V. 2014. Russian Federation Patent no 2558378 “Sposob opredeleniya maksimalnogo razmera por membrany” [A Method for Determining the Maximum Pore Size of the Membrane], March 5.
  7. Kolunin V. S., Ishkova Z. A. 2015. “Metod opredeleniya maksimalnogo razmera skvoznykh por keramiki po temperature nachala kristallizatsii vody” [A Method for Determining the Maximal Size of through Pores of Ceramics from the Temperature of the Water Crystallization Onset]. Pribory i tekhnika, no 5.
  8. Koopmans R. W. R., Miller R. D. 1966. “Soil freezing and soil water characteristic curves.” Soil Science Society of America, Proceedings, no 30, pp. 680-685.
  9. Plachenov T. G., Kolosentsev S. D. 1988. Porometriya [Porometry]. Leningrad: Khimiya.
  10. Tsytovich N. A. 1973. Mekhanika merzlykh gruntov [Mechanics of Frozen Soil]. Moscow: Vysshaya shkola.